Improving corrosion resistance of Al‐11mass%Si alloy through a large number of ECAP passes

Ultrafine‐grained (UFG) Al‐11mass%Si alloy, processed by multi‐pass equal‐channel angular pressing (ECAP) at 573 K, was investigated on corrosion behavior in 0.6 M NaCl solution. Potentiodynamic polarization tests and scanning electron microscopy observation showed that a large number of ECAP passes resulted in lower corrosion current density, more positive corrosion potential, and rather smooth corroded surface with shallow corrosion pits. The uniform distribution of fine secondary‐phase particles on UFG Al matrix weakened the susceptibility to pitting corrosion while inhibited general microgalvanic reactions. The present results indicate that grain refinement of aluminum matrix to the UFG state and uniform redistribution of broken particles (including eutectic silicon and secondary phases), via severe plastic deformation at elevated temperature undergoing dynamic recrystallization, can significantly improve the corrosion resistance of Al alloys, besides the known exceptional mechanical advantages. The simple and effective ECAP procedure makes UFG Al alloys more attractive for high strength structural application in corrosive environment.     

400MPa级细晶粒螺纹钢筋的生产开发

针对现有工艺设备,以20MnSi坯料为母材,通过调整化学成分,修改精轧孔型设计参数,采用控制轧制和控制冷却工艺,成功地生产铁素体晶粒尺寸在5～10μm的400 MPa级细晶粒钢筋。     

Synthesis of ultra-fine α-Al2O3 fibers via electrospinning method

Ultra-fine Al₂O₃ fibers were synthesized via electrospinning technique using PVP/ethanol polymer solution and aluminium acetate sol followed by calcinations at higher temperature. The formation, crystalline phase, surface morphology, fibers diameter and surface area of alumina ultra-fine fibers were characterized using FT-IR, TGA/DTA, XRD, SEM, TEM and BET analytical techniques. The results show that pure and crystalline α-Al₂O₃ ultra-fine fibers were formed with fiber diameter in the range of 100–500 nm and BET surface area of the fibers were found to be 40 m²/g.     

过量石灰对细粒土改良效果“负效应”机理的宏-细观试验研究

石灰是常用的特殊土改良材料,但掺量过大时反而导致改良土力学性质的劣化。为研究石灰掺量对细粒土改良效果“负效应”的产生机理,制备石灰掺杂质量分数为0%、3%、5%、7%、9%、11%的改良红砂岩残积土试样,分别养护28、60 d后进行无侧限抗压试验、扫描电子显微镜试验,获得无侧限抗压强度与石灰掺量和养护龄期的关系,以及不同石灰掺量改良土试样的微观结构特征。结果表明:对于本文试验中红砂岩残积土,无侧限抗压强度对应的最优石灰掺量为11%;石灰掺加质量分数不高于11%时,石灰充填在土颗粒孔隙中,起胶结土颗粒的作用,无侧限抗压强度提高;石灰掺加质量分数达到13%时,充填的石灰厚度过大,土颗粒“悬浮”在石灰之中,对承受轴向荷载的贡献大大减弱。     

阳泉一矿选煤厂180万t新增粒煤系统分析研究

针对阳泉一矿块煤产量小、易碎的实际情况,经过调研及多方论证,洗选产品增加了洗粒煤新产品,为企业取得了可观的经济效益。     

粗颗粒土橡皮膜嵌入试验研究

对于粗颗粒土三轴固结排水剪试验,橡皮膜嵌入是影响试验体变测量的最重要因素。通过在中三轴试样中埋置不同直径铁棒的方法进行等向固结试验来推求橡皮膜嵌入量。试验表明,试样土体体积与排水量呈较好的线性关系,基此给出了各个围压下的膜嵌入量。指出随着围压的增大,膜嵌入量逐渐增大,约0.8 MPa后,嵌入量的增速变缓,嵌入量占实时总排水量的比例可达31.0%~40.7%。由于粗颗粒土的各向异性,目前所用最多的Newland和Allely所提出的方法总体略高估了膜嵌入的大小,随着围压的增大,各向异性减弱,围压为2 MPa时嵌入量差异仅有0.22%的体变。最后,对比4种解析解发现Molenkamp和Luger的解析解最为接近试验值。针对粗颗粒土,需要进行更多的试验来建立颗粒破碎率和相对密度等与系数η的关系来修正解析解。     

细粒尾矿模袋充填体的特性试验研究

设计3个试验内容,分别从细粒尾矿、模袋体及模袋层间3个方面开展了细粒尾矿模袋法特性试验研究。研究表明,模袋与细粒尾矿组成的模袋充填体可获得较高的承载力,模袋层间强度参数较尾砂体亦有较大幅度的提高。最后开展现场工业试验,进一步揭示了细粒尾矿特性及其模袋法堆坝的适用性,拓宽了尾矿堆坝所要求的粒径范围。该成果对于进一步研究细粒尾矿模袋法堆坝具有指导意义。     

气流循环粉碎法制备Al2O3超细粉的研究

以粗颗粒Al2O3粉为原料,采用气流循环粉碎法制备了d50＜1μm的Al2O3超细粉.按正交表L9(34)安排正交试验,通过方差分析确定了制备Al2O3超细粉的最佳气流循环粉碎条件,并分析了各因素对气流循环粉碎过程的影响程度.不同物料的最佳气流循环粉碎条件应通过实验确定.在本研究的实验条件下,制备Al2O3超细粉的最佳条件为进气压力1.0 MPa,给料压力0.4 MPa,循环时间1.5 h.     

400MPa级超细晶粒钢焊接接头的低温韧性

利用CO2+Ar气体保护焊,分别采用单道焊接和双道焊接工艺对厚度为8 mm的400 MPa级超细晶粒钢钢板进行了焊接,采用系列冲击试验方法对焊接接头的低温韧性进行了研究。试验结果表明,在焊接接头中,焊逢位置低温韧性较差。由于双道焊较小的热输入,减小了焊缝及热影响区组织粗化,其焊接接头的低温韧性好于单道焊,并使热影响区面积变小。